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Title: Synthesis of a naphthalene-hydroxynaphthalene polymer model compound

Technical Report ·
DOI:https://doi.org/10.2172/6929711· OSTI ID:6929711

The objective of this project is the synthesis of a new naphthalene-hydroxynaphthalene polymer model compound for use in coal combustion studies. Since this compound is an unreported compound, this effort also requires the development of a synthetic route to this compound, including the synthesis of unreported intermediates leading to its synthesis. Complex product mixtures have been consistently obtained with all of our approaches. As a result, we have been constantly making small modifications to our technical approach. These changes are discussed in this report. Our synthesis efforts resulted in a number of potential precursors and intermediates. When appropriate, these compounds were submitted to the Organic Chemistry Research Area's Analytical Section for characterization and identification.

Research Organization:
Southern Research Inst., Birmingham, AL (United States)
Sponsoring Organization:
USDOE; USDOE, Washington, DC (United States)
DOE Contract Number:
AC22-90PC90038
OSTI ID:
6929711
Report Number(s):
DOE/PC/90038-T2; ON: DE93006127
Country of Publication:
United States
Language:
English