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Title: Liquefaction of sub-bituminous coal

Patent ·
OSTI ID:5479617

A process is described for the liquefaction of sub-bituminous coal, comprising: contacting sub-bituminous coal with a liquefaction solvent in a first stage thermal liquefaction zone; hydrogenating first stage product in a second stage with gaseous hydrogen, the second stage being operated at a temperature of no greater than 700/sup 0/F; recovering from the second stage a first stream of 850/sup 0/F- material, as net liquefaction product, and a second stream of a mixture of 850/sup 0/F- material and 850/sup 0/ F+ material; recovering a pumpable stream of insoluble material in 850/sup 0/F+ material from one of the first and second stage; and employing the pumpable stream and second stream for formulating liquefaction solvent for the first stage consisting essentially of from 5% to 10%, by weight, of insoluble material provided from one of the first and second stages, at least 45%, by weight, of 850/sup 0/F- material provided from the second stage without further hydrogenation, 0% to 20%, by weight, of 850/sup 0/F- material provided from the first stage without further hydrogenation, and the remainder of the liquefaction solvent being 850/sup 0/F+ material. The 850/sup 0/F+ material of the liquefaction solvent is provided in an amount of at least 20%, by weight, from the second stage without further hydrogenation and any remainder of the 850/sup 0/F+ material of the liquefaction solvent being provided from the first stage without further hydrogenation.

Assignee:
Lummus Crest, Inc., Bloomfield, NJ
Patent Number(s):
US 4596650
OSTI ID:
5479617
Resource Relation:
Patent File Date: Filed date 16 Mar 1984
Country of Publication:
United States
Language:
English