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Title: Retained austenite and tempered martensite embrittlement in medium carbon steels

Journal Article · · Metall. Trans., A; (United States)
DOI:https://doi.org/10.1007/BF02659860· OSTI ID:5440251

Electron microscopy, diffraction and microanalysis, X-ray diffraction, and auger spectroscopy have been used to study quenched and quenched and tempered 0.3 pct carbon low alloy steels. Some in sit fracture studies were also carried out in a high voltage electron microscope. Tempered martensite embrittlement (TME) is shown to arise primarily as a microstructural constraint associated with decomposition of interlath retained austenite into M/sub 3/C films upon tempering in the range of 250/sup 0/C to 400/sup 0/C. In addition, intralath Widmanstatten Fe/sub 3/C forms from epsilon carbide. The fracture is transgranular with respect to prior austenite. The situation is analogous to that in upper bainite This TME failure is different from temper embrittlement (TE) which occurs at higher tempering temperatures (approximately 500/sup 0/C), and is not a microstructural effect but rather due to impurity segregation (principally sulfur in the present work) to prior austenite grain boundaries leading t intergranular fracture along those boundaries. Both failures can occur in the same steels, depending on the tempering conditions.

Research Organization:
Memorex Corporation, Santa Clara, CA
DOE Contract Number:
AC03-76SF00098
OSTI ID:
5440251
Journal Information:
Metall. Trans., A; (United States), Vol. 14A
Country of Publication:
United States
Language:
English