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Title: Near-surface nucleation and crystallization of an ion-implanted lithia- alumina-silica glass

Journal Article · · J. Appl. Phys., v. 46, no. 10, pp. 4466-4473
DOI:https://doi.org/10.1063/1.321422· OSTI ID:4050919

Surface crystallization of a Au$sup +$-ion-implanted lithia-alumina- silica glass was realized. Annealing of a glass sample implanted with 285-keV Au$sup +$ ions at 550$sup 0$C results in the growth of colloidal Au particles of 18 to 35-A radius. The Au particles constitute sites for the precipitation of lithium metasilicate crystals at 550$sup 0$C. Further annealing at 750$sup 0$C allows the growth of quartz and $beta$-spodumene crystals. The crystallized surface obtained after the high-temperature anneal was characterized by a Knoop microhardness number of 626, which is of the order of that obtained for commercial volume-crystallized glass-ceramics of similar composition. (auth)

Research Organization:
Sandia Labs., Albuquerque, NM
Sponsoring Organization:
USDOE
NSA Number:
NSA-33-023831
OSTI ID:
4050919
Journal Information:
J. Appl. Phys., v. 46, no. 10, pp. 4466-4473, Other Information: Orig. Receipt Date: 30-JUN-76
Country of Publication:
United States
Language:
English