Characterization of phase development in non-isothermally annealed mould-cast and heat-treated Al-Mn-Sc-Zr alloys

Journal Article · Wed Dec 15 00:00:00 EST 2010 · Materials Characterization

DOI:https://doi.org/10.1016/J.MATCHAR.2010.10.006· OSTI ID:22063643

Vlach, M; Stulikova, I; Smola, B; Zaludova, N

The effect of Mn addition on microstructure and mechanical properties during isochronal annealing in the temperature range of 20 deg. C - 570 deg. C of the mould-cast and heat-treated Al-Sc-Zr alloys with a various content of Mn and Zr was studied. The electrical resistometry together with the microhardness (HV0.3) measurements were compared to microstructure development. The microstructure development was examined by scanning electron microscopy, transmission electron microscopy and electron diffraction. Relative resistivity changes and the microhardness of the mould-cast and heat-treated Al-Mn-Sc-Zr alloys exhibit similar dependence on annealing temperature. Precipitation of the Al{sub 3}Sc particles is responsible for the peak microhardness in all these alloys. The microhardness decrease is slightly delayed during the isochronal annealing and during the high temperature heat treatment in the mould-cast alloy with the higher Zr-content due to a higher oversaturation of Zr. The decomposition sequence of the oversaturated solid solution of the studied Al-Mn-Sc-Zr alloys is compatible with the recently published decomposition sequence of the Al-Sc-Zr system and also with the formation of Mn,Fe-containing particles. It seems very probable that the addition of Mn does not influence the decomposition of solid solution of the ternary Al-Sc-Zr system. - Research Highlights: {yields} Al{sub 3}Sc particles are responsible for the peak microhardness in all the studied alloys. {yields} The microhardness decrease is delayed in the alloy with the higher Zr-content. {yields} The peak hardening of the heat-treated alloys is shifted to higher temperatures. {yields} Mn does not influence the decomposition sequence of the Al-Sc-Zr system.

• OSTI ID: 22063643
• Journal Information: Materials Characterization, Vol. 61, Issue 12; Other Information: Copyright (c) 2010 Elsevier Science B.V., Amsterdam, The Netherlands, All rights reserved.; Country of input: International Atomic Energy Agency (IAEA); ISSN 1044-5803
• Country of Publication: United States
• Language: English

Related Subjects

36 MATERIALS SCIENCE
ALUMINIUM ALLOYS
ANNEALING
DECOMPOSITION
ELECTRIC CONDUCTIVITY
ELECTRON DIFFRACTION
HARDENING
MANGANESE ALLOYS
MICROHARDNESS
MICROSTRUCTURE
PARTICLES
PRECIPITATION
SCANDIUM ALLOYS
SCANNING ELECTRON MICROSCOPY
SOLID SOLUTIONS
TEMPERATURE DEPENDENCE
TRANSMISSION ELECTRON MICROSCOPY
ZIRCONIUM ALLOYS