Combined ultrasonic elastic wave velocity and microtomography measurements at high pressures
- Geodynamics Research Center, Ehime University, 2-5 Bunkyo-cho, Matsuyama 790-8577 (Japan)
- GeoSoilEnviroCARS, Center for Advanced Radiation Sources, University of Chicago, 5640 S, Ellis Avenue, Chicago, Illinois 60637 (United States)
Combined ultrasonic and microtomographic measurements were conducted for simultaneous determination of elastic property and density of noncrystalline materials at high pressures. A Paris-Edinburgh anvil cell was placed in a rotation apparatus, which enabled us to take a series of x-ray radiography images under pressure over a 180 deg. angle range and construct accurately the three-dimensional sample volume using microtomography. In addition, ultrasonic elastic wave velocity measurements were carried out simultaneously using the pulse reflection method with a 10 deg. Y-cut LiNbO{sub 3} transducer attached to the end of the lower anvil. Combined ultrasonic and microtomographic measurements were carried out for SiO{sub 2} glass up to 2.6 GPa and room temperature. A decrease in elastic wave velocities of the SiO{sub 2} glass was observed with increasing pressure, in agreement with previous studies. The simultaneous measurements on elastic wave velocities and density allowed us to derive bulk (K{sub s}) and shear (G) moduli as a function of pressure. K{sub s} and G of the SiO{sub 2} glass also decreased with increasing pressure. The negative pressure dependence of K{sub s} is stronger than that of G, and as a result the value of K{sub s} became similar to G at 2.0-2.6 GPa. There is no reason why we cannot apply this new technique to high temperatures as well. Hence the results demonstrate that the combined ultrasonic and microtomography technique is a powerful tool to derive advanced (accurate) P-V-K{sub s}-G-(T) equations of state for noncrystalline materials.
- OSTI ID:
- 22062255
- Journal Information:
- Review of Scientific Instruments, Vol. 82, Issue 2; Other Information: (c) 2011 American Institute of Physics; Country of input: International Atomic Energy Agency (IAEA); ISSN 0034-6748
- Country of Publication:
- United States
- Language:
- English
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Related Subjects
46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND TECHNOLOGY
CRYSTALS
ELASTICITY
EQUATIONS OF STATE
GLASS
IMAGES
LITHIUM COMPOUNDS
NANOSTRUCTURES
NIOBATES
PRESSURE DEPENDENCE
PRESSURE RANGE GIGA PA
PRESSURE RANGE MEGA PA 10-100
REFLECTION
SHEAR
SILICON OXIDES
TEMPERATURE RANGE 0273-0400 K
TEMPERATURE RANGE 0400-1000 K
TOMOGRAPHY
TRANSDUCERS
ULTRASONIC TESTING
X-RAY RADIOGRAPHY