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Title: Nanoparticle fabrication of hydroxyapatite by laser ablation in water

Journal Article · · Journal of Applied Physics
DOI:https://doi.org/10.1063/1.3000666· OSTI ID:21185876
; ; ;  [1];  [2]
  1. Department of Physics, University of Missouri-Kansas City, Kansas City, Missouri 64110 (United States)
  2. Department of Oral Biology, University of Missouri-Kansas City, Kansas City, Missouri 64110 (United States)

Synthetic polycrystalline hydroxyapatite was ablated in water with 337 nm radiation from a UV nitrogen pulsed laser. According to transmission electron microscopy micrographs, the ablated particles were approximately spherical and had a size of {approx}80 nm. Raman spectroscopic analysis demonstrated that particles had the same structure as the original crystal. X-ray photoelectron spectroscopy showed that the surface chemical composition was close to that of the original material. The characteristics of the ablated particles and estimations of the temperature rise of the hydroxyapatite surface under laser irradiation are consistent with the mechanism of explosive boiling being responsible for ablation. The experimental observations offer the basis for preparation of hydroxyapatite nanoparticles by laser ablation in water.

OSTI ID:
21185876
Journal Information:
Journal of Applied Physics, Vol. 104, Issue 8; Other Information: DOI: 10.1063/1.3000666; (c) 2008 American Institute of Physics; Country of input: International Atomic Energy Agency (IAEA); ISSN 0021-8979
Country of Publication:
United States
Language:
English