Phase Transition Dynamics in a Complex Oxide Heterostructure

Zhang, Qingteng; Hu, Guoxiang; Starchenko, Vitalii; Wan, Gang; Dufresne, Eric M.; Dong, Yongqi; Liu, Huajun; Zhou, Hua; Jeen, Hyoungjeen; Saritas, Kayahan; Krogel, Jaron T.; Reboredo, Fernando A.; Lee, Ho Nyung; Sandy, Alec R.; Almazan, Irene Calvo; Ganesh, Panchapakesan; Fong, Dillon D.

doi:10.1103/physrevlett.129.235701

Title: Phase Transition Dynamics in a Complex Oxide Heterostructure

Journal Article · Wed Nov 30 00:00:00 EST 2022 · Physical Review Letters

DOI:https://doi.org/10.1103/physrevlett.129.235701· OSTI ID:1969725

^[1]; Hu, Guoxiang ^[2]; Starchenko, Vitalii ^[3];

^[4];

^[1]; Dong, Yongqi ^[1];

^[5]; Zhou, Hua ^[1]; Jeen, Hyoungjeen ^[3];

^[3]; Krogel, Jaron T. ^[3]; Reboredo, Fernando A. ^[3]; Lee, Ho Nyung ^[3];

^[1]; Almazan, Irene Calvo ^[6]; Ganesh, Panchapakesan ^[7]; Fong, Dillon D. ^[1]

Argonne National Lab. (ANL), Lemont, IL (United States)
Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States). Center for Nanophase Materials Sciences (CNMS); City Univ. of New York (CUNY), NY (United States)
Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States)
Argonne National Lab. (ANL), Lemont, IL (United States); Stanford Univ., CA (United States)
Agency for Science, Technology and Research (A*STAR) (Singapore). Institute of Materials Research and Engineering
Argonne National Lab. (ANL), Lemont, IL (United States); University of Zaragoza (Spain). Institute of Nanosciences and Materials of Aragon (INMA)
Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States). Center for Nanophase Materials Sciences (CNMS)

Understanding the behavior of defects in the complex oxides is key to controlling myriad ionic and electronic properties in these multifunctional materials. The observation of defect dynamics, however, requires a unique probe-one sensitive to the configuration of defects as well as its time evolution. Here, we present measurements of oxygen vacancy ordering in epitaxial thin films of SrCoO_x and the brownmillerite-perovskite phase transition employing x-ray photon correlation spectroscopy. These and associated synchrotron measurements and theory calculations reveal the close interaction between the kinetics and the dynamics of the phase transition, showing how spatial and temporal fluctuations of heterointerface evolve during the transformation process. The energetics of the transition are correlated with the behavior of oxygen vacancies, and the dimensionality of the transformation is shown to depend strongly on whether the phase is undergoing oxidation or reduction. Finally, the experimental and theoretical methods described here are broadly applicable to in situ measurements of dynamic phase behavior and demonstrate how coherence may be employed for novel studies of the complex oxides as enabled by the arrival of fourth-generation hard x-ray coherent light sources.

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Research Organization:: Argonne National Laboratory (ANL), Argonne, IL (United States); Oak Ridge National Laboratory (ORNL), Oak Ridge, TN (United States). Oak Ridge Leadership Computing Facility (OLCF); Lawrence Berkeley National Laboratory (LBNL), Berkeley, CA (United States). National Energy Research Scientific Computing Center (NERSC); Oak Ridge National Laboratory (ORNL), Oak Ridge, TN (United States). Center for Nanophase Materials Sciences (CNMS)

Sponsoring Organization:: USDOE Office of Science (SC), Basic Energy Sciences (BES). Chemical Sciences, Geosciences & Biosciences Division; USDOE Office of Science (SC), Basic Energy Sciences (BES). Materials Sciences & Engineering Division; USDOE Office of Science (SC), Basic Energy Sciences (BES). Scientific User Facilities Division

Grant/Contract Number:: AC02-06CH11357; AC05-00OR22725; AC02-05CH11231

OSTI ID:: 1969725

Alternate ID(s):: OSTI ID: 1971034

Journal Information:: Physical Review Letters, Vol. 129, Issue 23; ISSN 0031-9007

Publisher:: American Physical Society (APS)Copyright Statement

Country of Publication:: United States

Language:: English

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