Water mediated growth of oriented single crystalline SrCO3 nanorod arrays on strontium compounds

Hong, Junsung; Heo, Su Jeong; Singh, Prabhakar

doi:10.1038/s41598-021-82651-0

Title: Water mediated growth of oriented single crystalline SrCO3 nanorod arrays on strontium compounds

Journal Article · Tue Feb 09 00:00:00 EST 2021 · Scientific Reports

DOI:https://doi.org/10.1038/s41598-021-82651-0· OSTI ID:1902561

Hong, Junsung; Heo, Su Jeong; Singh, Prabhakar

Abstract Morphology-controlled strontianite nanostructures have attracted interest in various fields, such as electrocatalyst and photocatalysts. Basic additives in aqueous strontium solutions is commonly used in controlling strontianite nanostructures. Here, we show that trace water also serves an important role in forming and structuring vertically oriented strontianite nanorod arrays on strontium compounds. Using in situ Raman spectroscopy, we monitored the structural evolution from hydrated strontium to strontianite nanorods, demonstrating the epitaxial growth by vapor–liquid–solid mechanism. Water molecules cause not only the exsolution of Sr liquid droplets on the surface but also the uptake of airborne CO ₂ followed by its ionization to CO ₃ ²⁻ . The existence of intermediate SrHO ⁺ –OCO ₂ ²⁻ phase indicates the interaction of CO ₃ ²⁻ with SrOH ⁺ in Sr(OH) _x (H ₂ O) _y cluster to orient strontianite crystals. X-ray diffraction simulation and transmission electron microscopy identify the preferred-orientation plane of the 1D nanostructures as the (002) plane, i.e., the growth along the c-axis. The anisotropic growth habit is found to be affected by the kinetics of carbonation. This study paves the way for designing and developing 1D architecture of alkaline earth metal carbonates by a simple method without external additives at room temperature.

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Research Organization:: Univ. of Connecticut, Storrs, CT (United States)

Sponsoring Organization:: USDOE

Grant/Contract Number:: FE-0023385; FE0023385

OSTI ID:: 1902561

Alternate ID(s):: OSTI ID: 1815499

Journal Information:: Scientific Reports, Journal Name: Scientific Reports Vol. 11 Journal Issue: 1; ISSN 2045-2322

Publisher:: Nature Publishing GroupCopyright Statement

Country of Publication:: United Kingdom

Language:: English

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