An algorithm for resolving intragranular orientation fields using coupled far-field and near-field high energy $\mathrm{X}$-ray diffraction microscopy

Nygren, Kelly E.; Pagan, Darren C.; Bernier, Joel V.; Miller, Matthew P.

doi:10.1016/j.matchar.2020.110366

Title: An algorithm for resolving intragranular orientation fields using coupled far-field and near-field high energy $$\mathrm{X}$$-ray diffraction microscopy

Journal Article · Mon May 11 00:00:00 EDT 2020 · Materials Characterization

DOI:https://doi.org/10.1016/j.matchar.2020.110366· OSTI ID:1888625

Nygren, Kelly E. ^[1]; Pagan, Darren C. ^[1]; Bernier, Joel V. ^[2]; Miller, Matthew P. ^[1]

Cornell University, Ithaca, NY (United States)
Lawrence Livermore National Lab. (LLNL), Livermore, CA (United States)

Here, we present a novel algorithm for reconstructing spatial intragranular lattice orientation fields using both far-field and near-field high energy X-ray diffraction microscopy (HEDM) measurements. An established far-field indexing algorithm is modified to include lattice orientation distribution information (grain orientation envelopes) in addition to average grain orientations. The near-field data reduction algorithm utilizes this enriched far-field orientation data as a seed for reconstructing intragranular spatial maps of lattice orientation from the diffraction images. The primary benefit of the new algorithm is a significant decrease in the number of trial calculations that must be performed in the reconstruction process compared to existing methodologies while maintaining scalability. The resulting gains in efficiency facilitate the use of relatively modest computational resources and improve throughput at the point of measurement. We provide two example applications: volumetric orientation field reconstructions for a Ti-Al alloy both before and after the application of 3% uniaxial strain. The results showcase the efficiency of the new method and the ability to resolve subtle changes in microstructure, which are associated with incipient plastic deformation.

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Research Organization:: Lawrence Livermore National Lab. (LLNL), Livermore, CA (United States)

Sponsoring Organization:: USDOE National Nuclear Security Administration (NNSA); US Department of the Navy, Office of Naval Research (ONR); National Science Foundation (NSF)

Grant/Contract Number:: AC52-07NA27344; N00014-16-1-2982; DMR-1829070

OSTI ID:: 1888625

Report Number(s):: LLNL-JRNL-839364; 1060318

Journal Information:: Materials Characterization, Vol. 165, Issue N/A; ISSN 1044-5803

Publisher:: ElsevierCopyright Statement

Country of Publication:: United States

Language:: English

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