Quantification of local dislocation density using 3D synchrotron monochromatic X-ray microdiffraction

Zhou, Guangni; Pantleon, Wolfgang; Xu, Ruqing; Liu, Wenjun; Chen, Kai; Zhang, Yubin

doi:10.1080/21663831.2020.1862932

Title: Quantification of local dislocation density using 3D synchrotron monochromatic X-ray microdiffraction

Journal Article · Mon Jan 11 00:00:00 EST 2021 · Materials Research Letters

DOI:https://doi.org/10.1080/21663831.2020.1862932· OSTI ID:1772097

Zhou, Guangni ^[1];

^[2]; Xu, Ruqing ^[3]; Liu, Wenjun ^[3];

^[4];

^[2]

Center for Advancing Materials Performance from the Nanoscale (CAMP-Nano), State Key Laboratory for Mechanical Behavior of Materials, Xi’an Jiaotong University, Xi’an, People’s Republic of China, Department of Mechanical Engineering, Technical University of Denmark, Kongens Lyngby, Denmark
Department of Mechanical Engineering, Technical University of Denmark, Kongens Lyngby, Denmark
Advanced Photon Source, Argonne National Laboratory, Lemont, IL, USA
Center for Advancing Materials Performance from the Nanoscale (CAMP-Nano), State Key Laboratory for Mechanical Behavior of Materials, Xi’an Jiaotong University, Xi’an, People’s Republic of China

A novel approach evolved from the classical Wilkens’ method has been developed to quantify the local dislocation density based on X-ray radial profiles obtained by 3D synchrotron monochromatic X-ray microdiffraction. A deformed Ni-based superalloy consisting of γ matrix and γ precipitates has been employed as model material. The quantitative results show that the local dislocation densities vary with the depths along the incident X-ray beam in both phases and are consistently higher in the γ matrix than in the γ precipitates. The results from X-ray microdiffraction are in general agreement with the transmission electron microscopic observations.

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Research Organization:: Argonne National Laboratory (ANL), Argonne, IL (United States)

Sponsoring Organization:: USDOE Office of Science (SC), Basic Energy Sciences (BES); National Natural Science Foundation of China (NSFC); National Key Research and Development Program of China; China Scholarship Council (CSC); Danish Council for Independent Research

Grant/Contract Number:: AC02-06CH11357; 91860109; 51671154; 51927801; 2016YFB0700404; 201806280355; 8022-00340B

OSTI ID:: 1772097

Alternate ID(s):: OSTI ID: 1840700

Journal Information:: Materials Research Letters, Journal Name: Materials Research Letters Vol. 9 Journal Issue: 4; ISSN 2166-3831

Publisher:: Informa UK LimitedCopyright Statement

Country of Publication:: United Kingdom

Language:: English

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36 MATERIALS SCIENCE
3D synchrotron microdiffraction
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dislocation density
transmission electron microscopy

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