Exploring Coupled Extreme Environments via In-situ Transmission Electron Microscopy

Parrish, Riley J.; Bufford, Daniel C.; Frazer, David M.; Taylor, Caitlin A.; Gutierrez-Kolar, Jacob; Buller, Daniel L.; Boyce, Brad L.; Hattar, Khalid

doi:10.1017/s1551929520001595

Title: Exploring Coupled Extreme Environments via In-situ Transmission Electron Microscopy

Journal Article · Fri Jan 15 00:00:00 EST 2021 · Microscopy Today

DOI:https://doi.org/10.1017/s1551929520001595· OSTI ID:1770788

Parrish, Riley J. ^[1]; Bufford, Daniel C. ^[1]; Frazer, David M. ^[2]; Taylor, Caitlin A. ^[3]; Gutierrez-Kolar, Jacob ^[1]; Buller, Daniel L. ^[1]; Boyce, Brad L. ^[1]; Hattar, Khalid ^[1]

Sandia National Lab. (SNL-NM), Albuquerque, NM (United States)
Idaho National Lab. (INL), Idaho Falls, ID (United States)
Sandia National Lab. (SNL-NM), Albuquerque, NM (United States); Los Alamos National Lab. (LANL), Los Alamos, NM (United States)

In-situ transmission electron microscopy (TEM) provides an avenue to explore time-dependent nanoscale material changes induced by a wide range of environmental conditions that govern material performance and degradation. The In-situ Ion Irradiation TEM (I³TEM) at Sandia National Laboratories is a JEOL 2100 microscope that has been highly modified with an array of hardware and software that makes it particularly well suited to explore fundamental mechanisms that arise from coupled extreme conditions. Here, examples pertaining to multibeam ion irradiation, rapid thermal cycling, and nanomechanical testing on the I³TEM are highlighted, along with prospective advancements in the field of in-situ microscopy.

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Research Organization:: Sandia National Lab. (SNL-NM), Albuquerque, NM (United States)

Sponsoring Organization:: USDOE National Nuclear Security Administration (NNSA); USDOE Office of Science (SC)

Grant/Contract Number:: AC04-94AL85000; AC07-051D14517; NA0003525

OSTI ID:: 1770788

Report Number(s):: SAND-2021-2560J; 694490

Journal Information:: Microscopy Today, Vol. 29, Issue 1; ISSN 1551-9295

Publisher:: Cambridge University PressCopyright Statement

Country of Publication:: United States

Language:: English

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