Permanent densification of silica glass for pressure calibration between 9 and 20 GPa at ambient temperature

Guerette, Michael; Poltorak, Alexandra; Fei, Yingwei; Strobel, Timothy A.

doi:10.1080/08957959.2019.1580364

Title: Permanent densification of silica glass for pressure calibration between 9 and 20 GPa at ambient temperature

Journal Article · Wed Jan 02 00:00:00 EST 2019 · High Pressure Research

DOI:https://doi.org/10.1080/08957959.2019.1580364· OSTI ID:1566671

^[1]; Poltorak, Alexandra ^[1]; Fei, Yingwei ^[1];

^[1]

Geophysical Laboratory, Carnegie Institution for Science, Washington, DC 20015, USA

Permanent density increase of silica glass was used to calibrate pressure generation delivered by cupped sintered diamond anvils (‘dimple anvils’) [Haberl B, Molaison JJ, Neuefeind JC, et al. Simple modified Bridgman anvil design for high pressure synthesis and neutron scattering. High Press. Res. submitted] within the Paris-Edinburgh press between approximately 9 and 20 GPa. Raman spectral changes of recovered silica glass with increased density were used to determine the maximum pressure reached by following an established calibration curve [Deschamps T, Kassir-Bodon A, Sonneville C, et al. Permanent densification of compressed silica glass: a Raman-density calibration curve. J. Phys. Condens. Matter. 2013;25:025402]. The monotonic Raman shift of the Main Band spectral region (~200–700 cm-1) of silica glass recovered from 9 to 20 GPa allows for continuous pressure calibration and is applicable to all presses that operate within this pressure range. Radial & axial Raman profiles were conducted to determine the pressure distribution within the sample chamber. This technique has been verified by in situ resistance measurements of the insulator-to-metal phase transition of ZnS near 15 GPa.

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Research Organization:: Energy Frontier Research Centers (EFRC) (United States). Energy Frontier Research in Extreme Environments (EFree); Carnegie Inst. of Washington, Washington, DC (United States)

Sponsoring Organization:: USDOE Office of Science (SC), Basic Energy Sciences (BES)

DOE Contract Number:: SC0001057

OSTI ID:: 1566671

Journal Information:: High Pressure Research, Vol. 39, Issue 1; ISSN 0895-7959

Publisher:: Taylor & Francis

Country of Publication:: United States

Language:: English

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Title: Permanent densification of silica glass for pressure calibration between 9 and 20 GPa at ambient temperature

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