NMR detector for supported monolayer and multilayer films
A novel NMR detector of the present invention comprises a radio frequency (RF) resonance circuit. The RF resonance circuit includes a principal detector element and a sample chamber. The principal detector element defines an inductor of the electronic resonance circuit. In one embodiment of the invention the sample chamber containing the inductor is a stainless steel sample chamber. The stainless steel sample chamber is a modified toroid cavity detector (TCD). The inductor is formed by an atomically flat metallic disk, such as, a mercury pool, with a predefined surface area, such as a surface area of 7.5 cm2. Liquid mercury is incorporated into a toroid cavity detector as the inductor of the resonance circuit, and as the base of the cavity. Self-assembled molecular structures (monolayers and multilayers) are formed using long-chain alkane thiols, which are known to chemically react with silver, gold, platinum, palladium, and mercury surfaces.
- Research Organization:
- Univ. of Chicago, IL (United States)
- Sponsoring Organization:
- USDOE
- DOE Contract Number:
- W-31-109-ENG-38
- Assignee:
- The University of Chicago (Chicago, IL)
- Patent Number(s):
- 6,791,326
- Application Number:
- 10/313,291
- OSTI ID:
- 1531482
- Resource Relation:
- Patent File Date: 2002-12-06
- Country of Publication:
- United States
- Language:
- English
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