A high-throughput energy-dispersive tender X-ray spectrometer for shot-to-shot sulfur measurements

Abraham, Baxter; Nowak, Stanislaw; Weninger, Clemens; Armenta, Rebecca; Defever, Jim; Day, David; Carini, Gabriella; Nakahara, Kazutaka; Gallo, Alessandro; Nelson, Silke; Nordlund, Dennis; Kroll, Thomas; Hunter, Mark S.; van Driel, Tim; Zhu, Diling; Weng, Tsu-Chien; Alonso-Mori, Roberto; Sokaras, Dimosthenis

doi:10.1107/S1600577519002431

Title: A high-throughput energy-dispersive tender X-ray spectrometer for shot-to-shot sulfur measurements

Journal Article · Tue Apr 02 00:00:00 EDT 2019 · Journal of Synchrotron Radiation (Online)

DOI:https://doi.org/10.1107/S1600577519002431· OSTI ID:1504514

Abraham, Baxter; Nowak, Stanislaw; Weninger, Clemens; Armenta, Rebecca; Defever, Jim; Day, David; Carini, Gabriella; Nakahara, Kazutaka; Gallo, Alessandro; Nelson, Silke; Nordlund, Dennis; Kroll, Thomas; Hunter, Mark S.; van Driel, Tim; Zhu, Diling; Weng, Tsu-Chien; Alonso-Mori, Roberto;

An X-ray emission spectrometer that can detect the sulfur Kα emission lines with large throughput and a high energy resolution is presented. The instrument is based on a large d-spacing perfect Bragg analyzer that diffracts the sulfur Kα emission at close to backscattering angles. This facilitates the application of efficient concepts routinely employed in hard X-ray spectrometers towards the tender X-ray regime. The instrument described in this work is based on an energy-dispersive von Hamos geometry that is well suited for photon-in photon-out spectroscopy at X-ray free-electron laser and synchrotron sources. Comparison of its performance with previously used instrumentation is presented through measurements using sulfur-containing species performed at the LCLS. It is shown that the overall signal intensity is increased by a factor of ∼15. Implementation of this approach in the design of a tender X-ray spectroscopy endstation for LCLS-II is also discussed.

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Research Organization:: Lawrence Berkeley National Laboratory (LBNL), Berkeley, CA (United States). National Energy Research Scientific Computing Center (NERSC); SLAC National Accelerator Laboratory (SLAC), Menlo Park, CA (United States)

Sponsoring Organization:: USDOE Office of Science (SC), Basic Energy Sciences (BES)

Grant/Contract Number:: AC02-76SF00515; AC02-05CH11231

OSTI ID:: 1504514

Alternate ID(s):: OSTI ID: 1527378; OSTI ID: 1528876

Journal Information:: Journal of Synchrotron Radiation (Online), Journal Name: Journal of Synchrotron Radiation (Online) Vol. 26 Journal Issue: 3; ISSN 1600-5775

Publisher:: International Union of CrystallographyCopyright Statement

Country of Publication:: Denmark

Language:: English

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Cited by: 11 works

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47 OTHER INSTRUMENTATION
36 MATERIALS SCIENCE
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photon-in photon-out spectroscopy methods

Title: A high-throughput energy-dispersive tender X-ray spectrometer for shot-to-shot sulfur measurements

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