Phase modulation due to crystal diffraction by ptychographic imaging

Civita, M.; Diaz, A.; Bean, R. J.; Shabalin, A. G.; Gorobtsov, O. Yu.; Vartanyants, I. A.; Robinson, I. K.

doi:10.1103/PhysRevB.97.104101

Title: Phase modulation due to crystal diffraction by ptychographic imaging

Journal Article · Tue Mar 06 00:00:00 EST 2018 · Physical Review. B

DOI:https://doi.org/10.1103/PhysRevB.97.104101· OSTI ID:1423915

Civita, M.; Diaz, A.; Bean, R. J.; Shabalin, A. G.; Gorobtsov, O. Yu.; Vartanyants, I. A.; Robinson, I. K.

Solving the phase problem in x-ray crystallography has occupied a considerable scientific effort in the 20th century and led to great advances in structural science. Here we use x-ray ptychography to demonstrate an interference method which measures the phase of the beam transmitted through a crystal, relative to the incoming beam, when diffraction takes place. The observed phase change of the direct beam through a small gold crystal is found to agree with both a quasikinematical model and full dynamical theories of diffraction. Our discovery of a diffraction contrast mechanism will enhance the interpretation of data obtained from crystalline samples using the ptychography method, which provides some of the most accurate x-ray phase-contrast images.

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Research Organization:: Brookhaven National Laboratory (BNL), Upton, NY (United States); Univ. College, London (United Kingdom)

Sponsoring Organization:: USDOE Office of Science (SC), Basic Energy Sciences (BES); Engineering and Physical Sciences Research Council (EPSRC)

Grant/Contract Number:: SC0012704; EP/I022562/1

OSTI ID:: 1423915

Alternate ID(s):: OSTI ID: 1425087

Report Number(s):: BNL-203280-2018-JAAM; PRBMDO; 104101

Journal Information:: Physical Review. B, Journal Name: Physical Review. B Vol. 97 Journal Issue: 10; ISSN 2469-9950

Publisher:: American Physical Society (APS)Copyright Statement

Country of Publication:: United States

Language:: English

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Cited by: 4 works

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75 CONDENSED MATTER PHYSICS
SUPERCONDUCTIVITY AND SUPERFLUIDITY
crystal phenomena
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coherent x-ray scattering
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Title: Phase modulation due to crystal diffraction by ptychographic imaging

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