Effect of coating thickness on interfacial shear behavior of zirconia-coated sapphire fibers in a polycrystalline alumina matrix
- Pennsylvania State Univ., University Park, PA (United States). Center for Advanced Materials
The effect of zirconia (ZrO{sub 2}) interfacial coatings on the interfacial shear behavior in sapphire reinforced alumina was examined in this study. Zirconia coatings of thicknesses ranging from 0.15 to 1.45 {mu}m were applied to single crystal sapphire (Saphikon) fibers using a particulate loaded sol dipping technique. After calcining at 1,100 C in air, the coated fibers were incorporated into a polycrystalline alumina matrix via hot pressing. Interfacial shear strength and sliding behavior of the coated fibers was examined using thin-slice indentation fiber pushout and pushback techniques. In all cases, debonding and sliding occurred at the interface between the fibers and the coating. The coatings exhibited a dense microstructure and led to a higher interfacial shear strength (> 240 MPa) and interfacial sliding stress (> 75 MPa) relative to previous studies on the effect of a porous interphase on interfacial properties. The interfacial shear strength decreased with increasing fiber coating thickness (from 389 {+-} 59 to 241 {+-} 43 MPa for 0.15 to 1.45 {micro}m thick coatings, respectively). Sliding behavior exhibited load modulation with increasing displacement during fiber sliding which is characteristic of fiber roughness-induced stick-slip. The high interfacial shear strengths and sliding stresses measured in this study, as well as the potentially strength degrading surface reconstruction observed on the coated fibers after hot pressing and heat treatment, indicate that dense zirconia coatings are not suitable candidates for optimizing composite toughness and strength in the sapphire fiber reinforced alumina system.
- OSTI ID:
- 100583
- Report Number(s):
- CONF-941144-; ISBN 1-55899-266-9; TRN: 95:019531
- Resource Relation:
- Conference: Fall meeting of the Materials Research Society (MRS), Boston, MA (United States), 28 Nov - 9 Dec 1994; Other Information: PBD: 1995; Related Information: Is Part Of Ceramic matrix composites -- Advanced high-temperature structural materials; Lowden, R.A.; Ferber, M.K. [eds.] [Oak Ridge National Lab., Oak Ridge, TN (United States)]; Hellmann, J.R. [ed.] [Pennsylvania State Univ., University Park, PA (United States). Center for Advanced Materials]; Chawla, K.K. [ed.] [New Mexico Inst. of Mining and Technology, Socorro, NM (United States)]; DiPietro, S.G. [ed.] [Textron Specialty Materials, Lowell, MA (United States)]; PB: 493 p.; Materials Research Society symposium proceedings, Volume 365
- Country of Publication:
- United States
- Language:
- English
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